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Appearance:powder
Throughput:100|Gram|Day
pd_productuse:air,sea and courier
Delivery Time:in stock
Purity:97% purity
Melting point 202 °C
Boiling point 270 °C (lit.)
density 1.071 g/mL at 25 °C (lit.)
refractive index n20/D 1.564(lit.)
Fp >230 °F
storage temp. Sealed in dry,Room Temperature
BRN 636823
CAS DataBase Reference 826-73-3(CAS DataBase Reference)
NIST Chemistry Reference 1-Benzosuberone(826-73-3)
Safety Information
Safety Statements 24/25
WGK Germany 3
HS Code 29143990
MSDS Information
Provider Language
1-Benzosuberone English
SigmaAldrich English
1-Benzosuberone Usage And Synthesis
Chemical Properties Light yellow liquid
Purification Methods Purify it by dissolving in toluene, washing with aqueous 5% NaOH, then brine, drying (MgSO4), and distilling. The 2,4-dinitrophenylhydrazone has m 210.5o, 207-208o (from CHCl3/MeOH). The Z-O-Picryloxime has m 156-157o (from Me2CO/MeOH), the E-O-picryloxime has m 107o. The oxime has m 106.5-107.5o. [UV: Gilmore & Horton J Am Chem Soc 73 1411 1951, Hedden & Brown J Am Chem Soc 75 3744 1953, Huisgen et al. Chem Ber 90 1844 1957, Beilstein 7 IV 1029.]
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